19.2 Process Equipment Selection, Sizing, and Optimization
Key Takeaways
- Vapor-liquid separator diameter follows the **Souders-Brown** relation \(v_{max} = K \sqrt{(\rho_L - \rho_V)/\rho_V}\), with \(K \approx 0.107\text{ m/s}\) (\(0.35\text{ ft/s}\)) for a vertical drum fitted with a mesh pad.
- Centrifugal pumps suit high flow, moderate head, and low viscosity; **positive displacement** pumps are required for high viscosity, low flow at high head, and metering duty, and they must never be operated against a closed discharge without a relief path.
- Centrifugal compressors suit high flow at moderate compression ratio; **reciprocating** compressors suit low flow at high compression ratio, and both are limited by discharge temperature, which forces multistaging with intercooling.
- Any capital-versus-operating optimum is found by setting \(dC_{total}/dx = 0\); when capital rises linearly and operating cost falls as \(1/x\), the optimum is \(x^* = \sqrt{a/b}\) and the **two cost terms are equal at the optimum**.
- Optimum reflux ratio for a distillation column lies at roughly **1.1 to 1.2 times \(R_{min}\)**, because column cost rises steeply as \(R \to R_{min}\) (infinite stages) while utility cost rises steadily as \(R\) increases.
19.2 Process Equipment Selection, Sizing, and Optimization
The NCEES specification names Process equipment design (e.g., equipment selection, optimization, sizing) under Design. Exam questions in this subtopic are short: pick the right machine for a stated duty, or size one piece of equipment from a standard correlation, or find the economic optimum of a single design variable.
1. Selection Logic
Pumps
| Duty | Choice | Why |
|---|---|---|
| High flow, moderate head, (\mu < 100\text{ cP}) | Centrifugal | Cheapest, simplest, smooth flow, throttleable |
| High viscosity ((> \sim 500\text{ cP})) | Positive displacement (gear, screw, progressing cavity) | Centrifugal head and efficiency collapse with viscosity |
| Low flow at high head | PD (reciprocating, plunger) | Centrifugal would need impractical impeller speed or staging |
| Accurate dosing | Metering (diaphragm) pump | Flow set by displacement, nearly independent of discharge pressure |
| Slurries | Recessed-impeller or peristaltic | Solids handling without trim damage |
The defining behavioral difference: a centrifugal pump produces a head that falls as flow rises, so closing the discharge simply drives it to shutoff head and it survives (briefly — it will overheat). A positive displacement pump produces whatever pressure it takes to move the fixed displacement, so closing the discharge ruptures the casing or the piping. Every PD pump requires a relief valve on the discharge, upstream of the first block valve.
Compressors
| Duty | Choice |
|---|---|
| High flow, compression ratio per stage (\lesssim 3) | Centrifugal |
| Low to moderate flow, high compression ratio | Reciprocating |
| Moderate flow, moderate ratio, dirty gas | Rotary screw |
| Very high flow, ratio (< 1.2) | Axial or blower |
Both types are limited by discharge temperature. For an ideal gas in isentropic compression, (T_2 = T_1 (P_2/P_1)^{(k-1)/k}), so compression ratio is capped by lubricant breakdown and by the material's temperature limit. This is why large ratios are split into multiple stages with intercooling, which also minimizes total work — the optimum stage pressure ratio for (n) stages with perfect intercooling is ((P_{final}/P_{initial})^{1/n}) at each stage.
Heat exchangers
| Situation | Choice |
|---|---|
| General duty, high pressure, large area | Shell and tube (Section 9.1) |
| Close temperature approach, clean fluids, moderate pressure | Plate-and-frame — approaches of (1-2^\circ\text{C}) are achievable |
| No cooling water available | Air-cooled — approach limited to (\sim 10-15^\circ\text{C}) above ambient |
| Small duty | Double-pipe / hairpin |
| Heavy fouling | Spiral, or shell-and-tube with removable bundle and generous fouling allowance |
2. Sizing a Vapor-Liquid Separator
Knockout drums, flash drums, compressor suction scrubbers, and reflux drums are all sized on the same principle: the upward gas velocity must be low enough that entrained droplets settle out rather than being carried over. Equating drag and gravity on a droplet gives the Souders-Brown equation:
| Configuration | (K) |
|---|---|
| Vertical drum with mesh pad mist eliminator | (\approx 0.107\text{ m/s}) ((0.35\text{ ft/s})) |
| Vertical drum without mist eliminator | (\approx 0.05-0.07\text{ m/s}) |
| Horizontal drum | Higher, because the gas path is longer relative to the settling distance |
Worked example. A vertical knockout drum with a mesh pad handles (2.0\text{ m}^3\text{/s}) of vapor at (\rho_V = 12\text{ kg/m}^3) with (\rho_L = 700\text{ kg/m}^3). Size the diameter.
Round up to a standard (1.8\text{ m}) shell. Height is then set separately by liquid holdup requirements (typically 5-10 minutes between high and low level for surge, more if the drum feeds a pump) plus disengagement space above the inlet nozzle and below the mesh pad.
Note the pressure sensitivity: (v_{max} \propto 1/\sqrt{\rho_V}) and (\rho_V \propto P), so a drum sized at (10\text{ bar}) and then operated at (20\text{ bar}) can handle a larger mass flow but a smaller volumetric one, and the same drum in vacuum service becomes enormous.
3. Economic Optimization of a Design Variable
Nearly every sizing decision is a contest between capital cost, which rises with size, and operating cost, which falls with size. The optimum is where the total is minimized:
The canonical form. When operating cost varies as (1/x) and annualized capital varies linearly with (x):
Example. Annual heat loss through insulation costs (a/x = 8{,}000/x) ($/\text{yr}) with (x) in inches, and annualized insulation capital is (bx = 500x) ($/\text{yr}). Then (x^* = \sqrt{8{,}000/500} = \sqrt{16} = 4.0\text{ in}), with (C_{min} = 8{,}000/4 + 500(4) = 2{,}000 + 2{,}000 = $4{,}000\text{/yr}).
Notice that at the optimum the two cost terms are exactly equal (($2{,}000) each). That equality is a property of this (1/x)-plus-linear form, and it makes a fast sanity check — but it does not generalize. For (C = a/x^2 + bx) the optimum has capital cost equal to twice the operating cost. Differentiate; do not assume.
The same structure recurs across the discipline:
| Design variable | Capital rises with | Operating falls with |
|---|---|---|
| Pipe diameter | More metal, larger valves and fittings | Lower velocity, less friction, less pump power |
| Insulation thickness | More insulation installed | Less heat loss |
| Exchanger approach (\Delta T) (smaller) | More area (as (1/\Delta T_{lm})) | Less utility consumed |
| Number of effects in an evaporator | More bodies | Less steam per unit evaporated |
| Reflux ratio | Fewer stages needed | — (utility cost rises with (R)) |
Optimum reflux ratio deserves its own note because it is shaped differently. As (R \to R_{min}) the required number of stages goes to infinity, so capital cost rises without bound; as (R) increases, stage count falls quickly at first and then flattens while reboiler and condenser duty (and column diameter) keep climbing. The total cost curve is therefore steep on the left and shallow on the right, and the minimum sits at roughly (R_{opt} \approx 1.1) to (1.2 \times R_{min}). Because the curve is flat near the optimum, designers commonly select toward the upper end to buy operating flexibility cheaply.
4. Heuristics Worth Carrying Into the Exam
These are the first-pass numbers a practicing process engineer uses before any rigorous calculation, and NCEES writes judgment questions against them:
- Liquid line velocity: (1-3\text{ m/s}) (pump discharge), (0.5-1.5\text{ m/s}) (pump suction, to protect NPSH).
- Gas line velocity: (15-30\text{ m/s}).
- Shell-and-tube (U): (\sim 850\text{ W/(m}^2\cdot\text{K)}) water-water, (\sim 300) organic-water, (\sim 30-60) gas-gas.
- Minimum exchanger approach: (\sim 10^\circ\text{C}) with cooling water, (\sim 5^\circ\text{C}) process-process, (1-2^\circ\text{C}) only in plate exchangers.
- Tray spacing (0.45-0.60\text{ m}); overall tray efficiency (50-70%) for hydrocarbons.
- Vessel L/D: (3) for low pressure, (4-5) at elevated pressure (shell cost favors slender vessels as pressure rises).
- Design margin: size equipment for roughly (110-120%) of design rate, and motors for the maximum possible operating point, not the normal one.
A vertical knockout drum fitted with a mesh pad (K = 0.107 m/s) must handle 3.5 m^3/s of vapor with vapor density 8.0 kg/m^3 and liquid density 640 kg/m^3. What minimum drum diameter is required?
A positive displacement metering pump is installed to dose catalyst into a reactor. During commissioning the discharge block valve is closed while the pump is running. What is the expected outcome, and what design feature should have prevented it?
The annual cost of a pipeline is modeled as C = 12,000/D + 3,000*D dollars per year, where D is the pipe diameter in inches, the first term representing pumping power and the second annualized capital. What is the economic diameter, and what does the total cost equal there?